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Beilstein J. Org. Chem. 2016, 12, 2570–2576, doi:10.3762/bjoc.12.252
Graphical Abstract
Scheme 1: Syntheses of the HCPs 3 and 5 via thiol–yne reaction.
Figure 1: IR-spectra of tetrathiol 2 (blue), tetraalkyne 1 (red) and HCP 3 (black).
Figure 2: IR-spectra of tetrathiol 2 (blue), hexaalkyne 4 (red) and HCP 3 (black).
Figure 3: SEM images of HCP 3 (left) and HCP 5 (right).
Figure 4: Adsorption isotherms of HCP 3 (green) and HCP 5 (blue) with nitrogen at 77 K. Desorption isotherms ...